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Linköping Institute of Technology

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Valid for year : 2009
 
NKEC16 Organic Analytical Chemistry, 12 ECTS credits.
/Organisk analytisk kemi/

For:   BKM   KA   Kem  

 

Prel. scheduled hours: 180
Rec. self-study hours: 140

  Area of Education: Science

Subject area: Chemistry

  Advancement level (G1, G2, A): G2

Aim:
To gain general and specific knowledge concerning the analysis of mainly low-molecular-weight organic compounds. The student will after the course cover many of the analytical techniques that are important within the field of chemical analysis. The student shall also be able to utilize scientific literature within the area. In order to achieve this it is necessary to:
  • Theoretically and practically cover gas chromatographic techniques
  • Theoretically and practically cover high performance liquid chromatographic techniques
  • Utilize mass spectrometry for the structural elucidation of unknown organic compounds
  • Treat samples before the final instrumental analysis
  • Develop analytical methods for trace element analysis, qualitatively as well as quantitatively


Prerequisites: (valid for students admitted to programmes within which the course is offered)
Analytical Chemistry T, Analytical Chemistry S, Analytical Chemistry K, Organic Chemistry 1, Organic Chemistry 2.

Note: Admission requirements for non-programme students usually also include admission requirements for the programme and threshhold requirements for progression within the programme, or corresponding.

Supplementary courses:
Forensic chemistry

Organisation:
Theory of mass spectrometry and chromatography are presented in lectures. Some lectures are devoted to spectrometric problem solving. In the laboratory the students use modern equipment for chemical separations and study their possibilities and limitations. Analytical methods for the analysis of environmental problems or consumption products are developed in groups of 2-3 students.

Course contents:
  • Mass spectrometry concerning the function of the spectrometer, the most common mass spectrometric techniques, manual and computerized interpretation of mass spectra and combinations of chromatographic separation techniques and mass spectrometry.
  • Chromatographic high resolution techniques. The development of analytical techniques in theory and practice. Trace element analysis regarding concentration, separation, identification and quantification.
Compulsory activities: All laborations and participation at educational visits.


Course literature:
H. Borén: Masspektrometri, Kompendium, LiU/IFM. S. Lindsay. High Performance Liquid Chromatography,Wiley. H.M. McNair and J.M. Miller: Basic Gas Chromatography, Wiley. Scientific publications.

Examination:
Written examination
Laboratory work
7 ECTS
5 ECTS
 
The examinations show in what respect the students fulfil the aims of the course. For passing, limitations regarding parts of the aims may be compensated by deeper knowledge of others.



Course language is Swedish.
Department offering the course: IFM.
Director of Studies: Stefan Svensson
Examiner: Roger Sävenhed

Course Syllabus in Swedish

Linköping Institute of Technology

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Contact: TFK , val@tfk.liu.se
Last updated: 08/28/2015